浩合元活性炭/吸附分離的實際應用

         純化(hua)中藥(yao)提(ti)取(qu)液的(de)應(ying)用應(ying)用大孔(kong)吸附(fu)樹脂分(fen)離，純化(hua)中藥(yao)提(ti)取(qu)液最(zui)早開始于(yu)七十(shi)年(nian)代末，到目前，在對中藥(yao)有(you)效成分(fen)的(de)分(fen)析以及中藥(yao)制(zhi)劑中的(de)應(ying)用都取(qu)得了(le)一些滿意的(de)結果’

中(zhong)(zhong)(zhong)(zhong)藥(yao)(yao)有效(xiao)(xiao)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)分(fen)(fen)析中(zhong)(zhong)(zhong)(zhong)的(de)(de)(de)(de)應用(yong)(yong)(yong)在(zai)對(dui)某(mou)(mou)些中(zhong)(zhong)(zhong)(zhong)藥(yao)(yao)材或者中(zhong)(zhong)(zhong)(zhong)藥(yao)(yao)復方(fang)制(zhi)劑中(zhong)(zhong)(zhong)(zhong)的(de)(de)(de)(de)有效(xiao)(xiao)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)進行定(ding)(ding)(ding)(ding)性、定(ding)(ding)(ding)(ding)量(liang)(liang)檢(jian)測(ce)(ce)(ce)(ce)(ce)時，使用(yong)(yong)(yong)大(da)孔(kong)(kong)(kong)吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)可(ke)有效(xiao)(xiao)的(de)(de)(de)(de)除(chu)去某(mou)(mou)些干擾(rao)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)，而取得(de)(de)較好的(de)(de)(de)(de)效(xiao)(xiao)果。據統(tong)計，用(yong)(yong)(yong)于(yu)皂(zao)甙(dai)(dai)(dai)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)的(de)(de)(de)(de)處(chu)(chu)理(li)報(bao)(bao)道甚多，用(yong)(yong)(yong)大(da)孔(kong)(kong)(kong)吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)純(chun)化供試品(pin)(pin)采(cai)(cai)用(yong)(yong)(yong)吸(xi)(xi)(xi)收光度法的(de)(de)(de)(de)有：章觀德測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)三(san)七(qi)及其(qi)(qi)制(zhi)劑冠(guan)心寧中(zhong)(zhong)(zhong)(zhong)的(de)(de)(de)(de)總(zong)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；董林(lin)等(deng)(deng)(deng)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)三(san)七(qi)蜂(feng)王漿(jiang)中(zhong)(zhong)(zhong)(zhong)三(san)七(qi)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；江林(lin)等(deng)(deng)(deng)對(dui)三(san)七(qi)全株不同(tong)生(sheng)長部位、不同(tong)規格、不同(tong)產地的(de)(de)(de)(de)22個樣(yang)(yang)品(pin)(pin)進行總(zong)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)；王乃(nai)利(li)等(deng)(deng)(deng)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)了(le)(le)國內外七(qi)種(zhong)人(ren)(ren)參(can)(can)根中(zhong)(zhong)(zhong)(zhong)及部分(fen)(fen)人(ren)(ren)參(can)(can)制(zhi)劑中(zhong)(zhong)(zhong)(zhong)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；張氏測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)西洋參(can)(can)蜂(feng)王漿(jiang)和人(ren)(ren)參(can)(can)蜂(feng)王漿(jiang)等(deng)(deng)(deng)口(kou)服(fu)液(ye)中(zhong)(zhong)(zhong)(zhong)總(zong)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；有人(ren)(ren)報(bao)(bao)道了(le)(le)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)氣(qi)血注(zhu)射(she)液(ye)、生(sheng)脈注(zhu)射(she)液(ye)、益氣(qi)活(huo)血沖劑等(deng)(deng)(deng)復方(fang)制(zhi)品(pin)(pin)中(zhong)(zhong)(zhong)(zhong)人(ren)(ren)參(can)(can)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)，也(ye)有吸(xi)(xi)(xi)附純(chun)化后(hou)采(cai)(cai)用(yong)(yong)(yong)薄(bo)層(ceng)掃(sao)(sao)描(miao)法測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)的(de)(de)(de)(de)，如(ru)：湯(tang)毅等(deng)(deng)(deng)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)西洋參(can)(can)口(kou)服(fu)液(ye)中(zhong)(zhong)(zhong)(zhong)人(ren)(ren)參(can)(can)皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；魏氏測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)補氣(qi)升提片中(zhong)(zhong)(zhong)(zhong)主要成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)人(ren)(ren)參(can)(can)皂(zao)甙(dai)(dai)(dai)Re的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；蘇子仁等(deng)(deng)(deng)測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)抗病毒口(kou)服(fu)液(ye)中(zhong)(zhong)(zhong)(zhong)知母皂(zao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)，除(chu)了(le)(le)皂(zao)甙(dai)(dai)(dai)以外，對(dui)于(yu)其(qi)(qi)他(ta)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)的(de)(de)(de)(de)檢(jian)測(ce)(ce)(ce)(ce)(ce)也(ye)相當成(cheng)(cheng)(cheng)(cheng)功，耿成(cheng)(cheng)(cheng)(cheng)國采(cai)(cai)用(yong)(yong)(yong)D型吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)分(fen)(fen)離比色(se)法測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)了(le)(le)甜葉菊中(zhong)(zhong)(zhong)(zhong)甜葉菊甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；壽國香等(deng)(deng)(deng)采(cai)(cai)用(yong)(yong)(yong)大(da)孔(kong)(kong)(kong)樹(shu)(shu)脂(zhi)(zhi)GDX104預分(fen)(fen)離，結(jie)合TLC雙波長掃(sao)(sao)描(miao)法測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)了(le)(le)疏(shu)肝止(zhi)痛(tong)片和消炎靈膠囊中(zhong)(zhong)(zhong)(zhong)芍藥(yao)(yao)甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；崔淑蓮(lian)等(deng)(deng)(deng)用(yong)(yong)(yong)大(da)孔(kong)(kong)(kong)吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)預處(chu)(chu)理(li)樣(yang)(yang)品(pin)(pin)后(hou)，再用(yong)(yong)(yong)HPLC法測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)祛瘀(yu)膠囊中(zhong)(zhong)(zhong)(zhong)橙皮甙(dai)(dai)(dai)的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)；朱宏紅等(deng)(deng)(deng)將樣(yang)(yang)品(pin)(pin)經(jing)大(da)孔(kong)(kong)(kong)吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)層(ceng)析處(chu)(chu)理(li)，再在(zai)聚酰胺薄(bo)膜(mo)上(shang)展開(kai)，定(ding)(ding)(ding)(ding)性檢(jian)測(ce)(ce)(ce)(ce)(ce)了(le)(le)痔康片中(zhong)(zhong)(zhong)(zhong)有效(xiao)(xiao)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)綠原酸，也(ye)有人(ren)(ren)采(cai)(cai)用(yong)(yong)(yong)樹(shu)(shu)脂(zhi)(zhi)分(fen)(fen)離一雙波長薄(bo)層(ceng)掃(sao)(sao)描(miao)法測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)了(le)(le)芪頤口(kou)服(fu)液(ye)中(zhong)(zhong)(zhong)(zhong)綠原酸的(de)(de)(de)(de)含(han)(han)(han)量(liang)(liang)，以上(shang)實驗表(biao)明(ming)：采(cai)(cai)用(yong)(yong)(yong)大(da)孔(kong)(kong)(kong)吸(xi)(xi)(xi)附樹(shu)(shu)脂(zhi)(zhi)對(dui)某(mou)(mou)些樣(yang)(yang)品(pin)(pin)在(zai)適當的(de)(de)(de)(de)條(tiao)件下進行預處(chu)(chu)理(li)，再結(jie)合其(qi)(qi)他(ta)的(de)(de)(de)(de)檢(jian)測(ce)(ce)(ce)(ce)(ce)手段測(ce)(ce)(ce)(ce)(ce)定(ding)(ding)(ding)(ding)其(qi)(qi)中(zhong)(zhong)(zhong)(zhong)的(de)(de)(de)(de)有效(xiao)(xiao)成(cheng)(cheng)(cheng)(cheng)分(fen)(fen)，不僅結(jie)果準確、可(ke)靠，而且(qie)對(dui)控制(zhi)中(zhong)(zhong)(zhong)(zhong)藥(yao)(yao)材和中(zhong)(zhong)(zhong)(zhong)藥(yao)(yao)制(zhi)劑的(de)(de)(de)(de)質(zhi)量(liang)(liang)具有很好的(de)(de)(de)(de)實用(yong)(yong)(yong)價值(zhi)，值(zhi)得(de)(de)借鑒推廣。